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Table 1 Materials used and treatment protocol

From: Efffect of desensitizing agents on the bond strength of dental adhesive systems

Material

Composition

Protocol

Manufacturer

Adper Scotchbond Multiuse adhesive system

Primer: HEMA, polyalkenoic acid.

a) phosphoric acid (37%): 15 sec.

3 M ESPE, St Paul, USA

b) tap water: 15 sec.

c) removal of excess moisture with paper towel.

Bond: Bis-GMA, HEMA and amines.

d) primer

e) air jet: 5 sec. (distance 10 cm)

f) adhesive

g) photoactivation: 10 seconds.

Clearfil SE Bond adhesive system

Primer: MDP, HEMA, camphorquinone, hydrophilic dimethacrylate, N, N-diethanol P-toluidine and water.

a) primer: rubbing for 20 sec.

Kuraray Medical Inc, Tokyo, Japan.

b) air jet: 10 sec. (distance 10 cm)

Bond: MDP, BIS-GMA, HEMA, hydrophobic aliphatic dimethacrylate, camphorquinone, N, N-diethanol-P-toluidine, silanized colloidal silica.

c) adhesive

d) air jet: 10 sec. (distance 10 cm)

e) photoactivation: 10 sec.

Colgate Sensitive Pro-Relief Paste

Calcium carbonate, hydrated silica, glycerin, arginine, water, sodium bicarbonate, fragrance, sodium carboxymethylcellulose, sodium saccharin, blue 1(Cl 42090).

a) application with impregnated rubber cup at low speed for 3 sec.

Palmolive Company, New York, USA

b) rinse with deionized water

c) repeat procedure

Aqueous Biosilicate® solution (10%)

Bioglass mixed with distilled water (ratio 1:10).

a) application and rubbing of solution on dentin for 30 sec.

Vitrovita, São Carlos, Brazil.

b) wait: 3 min.

c) remove excess: air jet

d) repeat procedure

e) rinse with deionized water