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Applied Adhesion Science

Table 1 Materials used in this study

From: Influence of solvent evaporation on ultimate tensile strength of contemporary dental adhesives

Adhesive (manufacturer)

Ingredients

Batch no.

2-step self-etch adhesive

 Clearfil SE Protect (Kuraray Noritake Dental)a

Bis-GMA, HEMA, 10-MDP, Hydrophobic aliphatic methacrylate, colloidal silica, CQ, initiators and accelerators, sodium fluoride, others

CK0014

 OptiBond XTR (Kerr)

Hydrophobic monomers, ethanol, camphorquinone, 0.4-μm barium glass, nano-silica filler, sodium hexafluorosilicate

5143490

1-step self-etch adhesive

 OptiBond All-In-One (Kerr)

GPDM, glycerol dimethacrylate, HEMA, water, acetone, ethanol, CQ-based photo-initiator, nano-sized fillers, sodium hexafluorosilicate, ytterbium fluoride

5164557

 G-Premio Bond (GC)

4-MET, MDP, MDTP, methacrylate monomer, acetone, water, photo initiators, silica

1605241

  1. Bis-GMA, 2,2-bis[4-(2-hydroxy-3-methacryloyloxypropoxy)phenyl]propane; CQ, dl-camphorquinone; GPDM, glycerol-phosphate-dimethacrylate; HEMA; hydroxyethylmethacrylate; 4-MET, 4-methacryloyloxyethyl trimellitate; 10-MDP, methacryloyloxydecyl dihydrogen phosphate; MDTP, methacryloyloxydecyl dihydrogen thiophosphate
  2. aAlso known as “Clearfil Megabond FA” in Japan
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