Effect of surface roughness using different adherend materials on the adhesive bond strength
© Budhe et al. 2015
Received: 24 November 2015
Accepted: 8 December 2015
Published: 14 December 2015
In this paper, an experimental study on the effect of surface roughness of different adherend material on adhesive bond strength was carried out. The adherend material used was aluminium AA6061 and wood in the form of sheet, and the adhesive was an epoxy resin. Different surface roughness obtained by mechanical abrasion using an emery paper and sand paper for aluminium and wood adherend samples respectively. Single strap joints were tested at room temperature. Results showed that there is clear dependency observed in between the adhesive bond strength and surface roughness of both wood and aluminium adherend joints. Optimum surface roughness values were obtained in the range of Ra = 1.68 ± 0.14 µm and Ra = 1.64 ± 0.2 µm for the aluminium and wood adherend joints respectively. Surface roughness along with the adhered material parameters should be considered during design stage of adhesively bonded joints.
KeywordsAdhesive bond strength Surface roughness Adherend material Single strap joint
Mechanical performance of adhesive bonded joints depends on a number of parameters such as: material properties and joint geometry (adhesive thickness, adherend thickness), surface roughness etc. . Therefore these parameters have a great importance in industrial application for achieving maximum strength. During the design of adhesively bonded joints, one has to take into account these factors associated with the bond strength. A number of researchers [2–6] have examined the effect of different parameters on the strength and durability of adhesive joints. The nature of the adherends has highly influence on the strength of the adhesive bond.
Surface roughness is one of the important factors which influence the mechanical properties of the joints. The relationship between the surface roughness and adhesion is very complex. Most of the researchers [7–9] noticed the importance of surface and its positive influence on the bond strength. There are different surface treatments methods available such as grinding, grit blasting, mechanical etching, plasma, chemical etching etc. Critchow and Brewis  studied the influence of adherend surface roughness on the durability of adhesive bonding joints. Surface roughness was achieved by grit blasting method. They observed that roughness has a significant effect on durability of epoxy-Al joint. Dayss et al.  investigated the effect of surface roughness of polymer adherend on adhesive bond strength. Mechanical grinding and low-pressure plasma treatment was used for modifying surface properties. It was found that increased roughness led to improvement in bond strength, but there was a limit of around 1 MPa. Tezcan et al.  studied the effect of surface roughness on the strength of adhesive bond under static and dynamic conditions. It was observed that low roughness values gave the lowest static strength and load cycle values. For roughness values of Ra = 1.5 to 2.5 μm, the static strength showed a decreasing trend while from Ra = 0.5 to 2 μm, the highest number of load cycles were obtained. Baburaj et al.  noticed an enhancement of adhesive joint strength by laser surface modification. Uehara  concluded that an optimum surface roughness value exist for the maximum tensile strength. However, no clear relationship was observed between the peel strength and the surface roughness. Zhang et al.  investigated the effect of surface pre-treatment on adhesive properties of aluminium alloys. They found that maximum lap shear strength and durability of adhesive bonding joints can be improved by surface treatment and roughness modification. On the other hand, the surface roughness of wood is influenced to a much higher degree by environmental factors such as temperature, humidity etc. than a metallic structural material like aluminum. For wood adherend joints, the lower surface roughness value (smoother surface) gives the higher bond strength joint [15, 16].
As summarized above, there is no general trend which relates the surface roughness with the strength of adhesive bonded joints. An optimum surface roughness range is differing with respect to the adhesive-adherend combinations in order to get high performance of bonded joints. Therefore, for different adhesive-adherend joints, there will be a different optimum range of roughness with regard to bond strength. It is of interest to study the change in behaviour of adhesively bonded joint with change in adherend material. The objective of the present study is to investigate the influence of surface roughness using aluminium and wood adherend material on the adhesive bond strength.
Chemical composition and mechanical properties of Aluminium AA6061
Chemical composition (%)
Ultimate tensile strength (MPa)
Yield strength (MPa)
The surface roughness of the aluminium adherend was varied by mechanical abrasion using an emery paper. Different grades of emery paper identified by P120, P50 and P30 were used to produce different levels of surface roughness and as-purchased aluminium plate surface roughness was itself used as one grade. The residual particles remaining after mechanical abrasion were removed by cleaning the surface with a soft clean cloth. For wood adherends, the surface roughness was varied by mechanical abrasion using sand paper. Different grades of sand paper identified by P120, P80 and P50 were used to produce different level of surface roughness and wood billet after planning operation was itself used as a one grade.
Surface roughness of treated and untreated samples was measured using a profilometer (Pocket Surf Make Mahr, GMBH, Model EMD 1500). The measuring range of the profilometer was 0.03–6.35 μm, while the sensor traversing length for all cases was 10 mm. Two roughness parameters, namely average roughness (Ra) and maximum roughness (maximum height of profile, Rz) were used to evaluate surface roughness of the specimens. Measurements were performed in different areas, along two different mutually perpendicular directions, longitudinal and tangential.
Results and discussions
Surface roughness and shear strength values
Surface roughness value of aluminium adherend
0.54 ± 0.15
3.75 ± 1.25
1.68 ± 0.14
10.27 ± 2.50
2.69 ± 0.17
17 ± 1.68
3.66 ± 0.13
23.5 ± 2.0
Surface roughness value of wood adherend
1.64 ± 0.20
9.2 ± 1.55
2.63 ± 0.19
15.75 ± 2.20
3.37 ± 0.18
21.2 ± 1.70
4.11 ± 0.22
25.24 ± 1.90
Significant increase in bonding strength (i.e. 26.70 %) is achieved by maintaining surface roughness values in the range of 1.68 ± 0.14 μm as compared to surface without treatment (0.54 ± 0.15 μm). In this range there would be an optimal point where can get a maximum bonding strength. An increase in surface area, mechanical locking adhesive between micro columns, and modification in the surface chemistry of the adherend are the possible reasons for the improvement in the bond strength at higher surface roughness as compared to the smooth surface [8, 13].Some author [11, 17] observed that an insufficient wetting occur at higher surface roughness and that might be the reason for lower bond strength, when surface roughness value are beyond 2.5 μm (Ra > 2.5 μm).
To conclude, the trend of bonding strength of aluminium and wood adherend are totally different and it depends on the type of adherend materials. The maximum strength can be obtained for the optimum surface roughness value of respective combination of adherend adhesive materials.
Linear regression analysis
The entire experimental data of aluminium adherend joints are divided into two groups. First group consist of original surface of aluminium adherend and varied by the mechanical abrasion using emery paper of P120 grade. The surface roughness of the aluminium adhered was varied by the mechanical abrasion using emery paper of P50 and P30 grade, considered as the second group. The roughness value ranging from 0.41 to 1.78 μm in first group and from 2.59 to 3.74 μm in second group also called lower and higher roughness group respectively. There are 14 pairs of data in the lower roughness group and 13 pairs of data in the higher roughness group.
Equations (1) and (2) were obtained by performing a regression analysis on the experimental data for aluminium adherend joints.
The fitted curves are shown in Fig. 5. The coefficient of correlation estimate R2 is 0.974 for the first group of data, and 0.84 for the second group. Without performing any additional experiments, Eqs. 1 and 2 can be used to calculate approximate shear stress for the surface roughnessvalues between Ra = 0.41 to 1.78 μm and Ra = 2.59 to 3.74 μm respectively. However, these equations are valid for the specific adherend-adhesive combinations i.e. Aluminium AA6061 and araldite® 2015 adhesive only.
Equation (3) was obtained by performing a regression analysis on the entire experimental set of data for wood adherend joints.
From Fig. 6, it can be seen that the maximum strength was achieved for the lower surface roughness value of wood adherend. As the surface roughness value increased, the bonding strength decrease and vice versa. Bond strength of smooth adherend surface is higher than that of rough one for the wood adhesive bonded joints.
Adhesive joints with aluminium and wood adherend were fabricated and tested in order to study the effect of varying surface roughness of adherend on adhesive bond strength.
Optimum surface roughness value was found in the range of 1.75–2.5 μm for the maximum bond strength of aluminium adherend joints. The lower bonding strength was obtained for both lower surface roughness (Ra < 1.68 ± 0.14 μm) and very high surface roughness (Ra > 2.69 ± 0.17 μm) also. The adhesive bond strength varies with respect to the surface roughness of adherend.
Mixed failure between the adherend and adhesive occurred when the adherend had lower surface (0.54 ± 0.15) and then failure mode partially shift towards the cohesive failure mode close to interface when the surface roughness increases. Cohesive failures along with the mechanical interlocking phenomenon are the possible explanation for the variation in bonding shear strength.
The adhesive bond strength decreases continuously with increase in adhered surface roughness of wood adherend. The maximum bond strength was obtained for the smooth wood adherend surface (Ra = 1.64 ± 0.25 μm).
Failure mode shifted from adhered failure mode to mixed failure mode as the surface roughness of wood adherend increased from 1.64 to 4.11 μm.
The surface roughness parameter must be considered during the design stage of adhesively bonded joints, as the bond strength varied significantly by 30–40 %, between the different surface roughness values.
SB (First and corresponding author) was responsible for completing article and guiding to my master student for the experimental work of this paper and discuss results with all authors. AG participated in the experimental works from the purchasing of material to sample preparation and testing of the specimens. NB carried out the data regression analysis and the surface failure analysis of the fracture specimens. MB carried out analysing the failure mode of the fractured specimen, results discussion and great contribute to making final draft of the article. All authors read and approved the final manuscript.
The authors declare that they have no competing interests.
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- Banea MD, Da Silva LFM. Adhesively bonded joints in composite materials: an overview. J Mater Design Appl. 2009;223:1–18. doi:https://doi.org/10.1243/14644207JMDA219.Google Scholar
- Critchow GW, Brewis M. Influence of surface macro roughness on the durability of epoxies-Al joints. Int J Adhes Adhes. 1995;15(3):173–6. doi:https://doi.org/10.1016/0143-7496(95)91628-J.View ArticleGoogle Scholar
- Korkut DS, Korkut S, Bekar I, Budakci M, Dilik T, Cakicier N. The effect of heat treatment on physical properties and surface roughness of Turkish Hazel. Int J Mol Sci. 2008;9(9):1772–83. doi:https://doi.org/10.3390/ijms9091772.View ArticleGoogle Scholar
- Da Silva LFM, Carbas RJC, Critchlow GW, Figueiredo MAV, Brown K. Effect of material, geometry, surface treatment and environment on the shear strength of single lap joints. Int J Adhes Adhes. 2009;29(6):621–32. doi:https://doi.org/10.1016/j.ijadhadh.2009.02.012.View ArticleGoogle Scholar
- Pereira AM, Ferreira JM, Antunes FV, Bártolo PJ. Analysis of manufacturing parameters on the shear strength of aluminium adhesive single-lap joints. J Mater Process Technol. 2010;210(4):610–7. doi:https://doi.org/10.1016/j.jmatprotec.2009.11.006.View ArticleGoogle Scholar
- Kahraman R, Sunar M, Yilbas B. Influence of adhesive thickness and filler content on the mechanical performance of aluminium single-lap joints bonded with aluminum powder filled epoxy adhesive. J Mater Process Technol. 2008;205(1):183–9. doi:https://doi.org/10.1016/j.jmatprotec.2007.11.121.View ArticleGoogle Scholar
- Lonardo PM, Bruzzone AAG. Influence of surface roughness parameters on the mechanical strength in metal gluing. CIRP Ann Manuf Technol. 1989;38(1):571–4. doi:https://doi.org/10.1016/S0007-8506(07)62771-1.View ArticleGoogle Scholar
- Sahid M, Hashim SA. Effect of surface roughness on the strength of cleavage joints. Int J Adhes Adhes. 2002;22(3):235–44. doi:https://doi.org/10.1016/S0143-7496(01)00059-8.View ArticleGoogle Scholar
- Benard Q, Fois M, Grisel M. Peel ply surface treatment for composite assemblies: chemistry and morphology effects. Compos A. 2005;36(11):1562–8. doi:https://doi.org/10.1016/j.compositesa.2005.02.012.View ArticleGoogle Scholar
- Dayss E, Leps G, Meinhardt J. Surface modification for improved adhesion of a polymer-metal compound. J Surf Coat Technol. 1999;116–119:986–90. doi:https://doi.org/10.1016/S0257-8972(99)00184-X.View ArticleGoogle Scholar
- Sekercioglu T, Rende H, Gulsoz A, Meran C. The effect of surface roughness on strength of adhesively bonded cylindrical components. J Mater Process Technol. 2003;142(1):82–6. doi:https://doi.org/10.1016/S0924-0136(03)00463-1.View ArticleGoogle Scholar
- Baburag EG, Stariko D, Evans J, Shafeev GA, Bensaoulo A. Enhancement of adhesive joint strength by laser surface modification. Int J Adhes Adhes. 2007;27(4):268–76. doi:https://doi.org/10.1016/j.ijadhadh.2006.05.004.View ArticleGoogle Scholar
- Uehara K, Sakurai M. Bonding strength of adhesives and surface roughness of joined parts. J Mater Process Technol. 2002;127(2):178–81. doi:https://doi.org/10.1016/S0924-0136(02)00122-X.View ArticleGoogle Scholar
- Zhang J, Zhao X, Zuo Y, Xiong J, Zhang X. Effect of surface pretreatment on adhesive properties of aluminium alloys. J Mater Sci. 2007;24:236–40. http://www.jourlib.org/paper/1534092#.Vl8SnXarSM8.
- Ozdemir T, Hiziroglu S, Malkocoglu A. Influence of relative humidity on surface quality and adhesion strength of coated medium density fibreboard panels. Mater Design. 2009;30(7):2543–6. doi:https://doi.org/10.1016/j.matdes.2008.09.036.View ArticleGoogle Scholar
- Sulaiman O, Hashim R, Subari K, Liang CK. Effect of sanding on surface roughness of rubber wood. J Mater Process Technol. 2008;209(8):3949–55. doi:https://doi.org/10.1016/j.jmatprotec.2008.09.009.View ArticleGoogle Scholar
- Borsellino C, Bella GD, Ruisi VF. Adhesive joining of aluminium AA6082: the effects of resin and surface treatment. Int J Adhes Adhes. 2008;29:36–44. doi:https://doi.org/10.1016/j.ijadhadh.2008.01.002.View ArticleGoogle Scholar
- Murmanis L, River BH, Stewart H. Microscopy of abrasive-planed and knife-planed surfaces in wood–adhesive bonds. Wood Fiber Sci. 1983;15(2):102–15. http://wfs.swst.org/index.php/wfs/article/view/1181.